KMID : 1059519850290030311
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Journal of the Korean Chemical Society 1985 Volume.29 No. 3 p.311 ~ p.318
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Synthesis of 1-[3-(Propylthio)butyryl]-2,6,6-trimethylcyclohexene
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Oh Jong-Hoon
Kim Kyong-Tae Kim Yong-Tae
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Abstract
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1-[3-(Propylthio)butyryl]-2,6,6-trimethylcyclohexene (18) was synthesized from the reaction of 2,6,6-trimethylcyclohex-l-en-1-yllithium (9) with 3-propylthiobutyraldehyde (16). This method will be employed to prepare 1-[3-(methylthio)butyryl]-2,6,6-trimethylcyclohexene (1) which is known as one of the powerful flavors and fragrances.
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